Procedures for Microwave Activated Supported Reagent Dry Media Reactions:

General Information: Reactions were run using 8 mL polypropylene SPE reservoirs obtained from Alltech Associates. The microwave oven was a 600 watt model from Emerson Electric. All chemicals can be obtained from Aldrich Chemical Company. The HPLC analyses were performed using a 4 mm x 10 cm Phase-Sep C-18 column and a mobile phase of 50% MeOH / 50% water. The gas chromatographic analyses were performed using a Gow-Mac instrument and a 5' x 1/8" OV 101 silicone column.

 

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